HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 23675389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 14349173 | HCID 14349173 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23675389 | HCID 23675389 | — |
Reaction Steps
In 5 ml of ethanol was dissolved in 1.40 g of ethyl 2,2-dimethyl-5-[p-(2-methyl-4-thiazolyl)phenoxy]pentanoate obtained in EXAMPLE 5. The solution was added to an aqueous sodium hydroxide solution (0.4 g of sodium hydroxide in 5 ml of water) and the mixture refluxed for 10 hours. After cooling, the precipitated crystals was washed with water to obtain the desired product, sodium 2,2-dimethyl-5-[p-(2-methyl-4-thiazolyl)phenoxy]pentanoate as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04794113 |
| Source dataset | uspto-grants-1988_12 |
| ORD ID | ord-e9dff706ab2d448082dceaf2421351e0 |
| Source note | uspto-grants-1988_12 |