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HRID414750

反应详情

EQUATION

反应方程式

HRID 414750 的结构方程式

REACTANTS

反应物

2
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：O=C(O)CCCCn1cnnn1
HCID21280290

5-(1H-Tetrazol-1-yl)pentanoic acid

C6H10N4O2

PRODUCTS

生成物

1
结构：O=C(Cl)CCCCn1cnnn1
HCID17803406

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CN(C)C=O
催化剂HCID6228

N,N-Dimethylformamide

C3H7NO

结构：c1ccccc1
溶剂HCID241

Benzene

C6H6

PROCEDURE

实验过程

1 g of 5-(tetrazol-1-yl)-valeric acid is heated for 20 minutes at reflux temperature in 12 ml of absolute benzene with 0.6 ml of thionyl chloride and 2 drops of DMF. After concentration by evaporation under reduced pressure, the title compound is obtained.

WORKUP

后处理

  1. concentrationAfter concentration
  2. customby evaporation under reduced pressure