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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 414836Generated: October 30, 2026

Methanol → HCID 14349152, compound

https://huagongshe.com/reaction/414836

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantPhenolHCID 996—
ReactantDibenzyl etherHCID 7657—
CatalystPalladiumHCID 23938—
ProductHCID 14349152HCID 1434915283%

Reaction Steps

The benzyl ether of the desired phenol (26 g) was taken in methanol (150 ml) and this solution was hydrogenated in a Parr apparatus under an atmosphere of hydrogen (45-50 lbs./sq.in.) in the presence of 10% palladium on charcoal (10 g). After 20-24 hours, the suspension was filtered on celite; all methanol was removed to obtain the desired phenol in about 83% yield (15.4 g) as a coloress liquid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04794188
Source datasetuspto-grants-1988_12
ORD IDord-ea4a23cde1f74e8fbace4d17864417bf
Source noteuspto-grants-1988_12