HRID415211
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To the mixture of methyl 2-(4-(bromomethyl)phenyl)benzo[d]oxazole-7-carboxylate (250 mg, 0.72 mmol) in methanol (2 mL), was added piperazine (186 mg, 2.16 mmol), and the resulting mixture was stirred at room temperature for 17 hr, then the solvents were evaporated to give methyl 2-(4-(piperazin-1-ylmethyl)phenyl)benzo[d]oxazole-7-carboxylate LC-MS (ESI) m/z 352 [M+1]+.
WORKUP
后处理
- customthe solvents were evaporated