HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-((Trifluoromethyl)thio)aniline → HCID 66619688, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-((Trifluoromethyl)thio)aniline | HCID 2735939 | — |
| Reactant | HCID 13265891 | HCID 13265891 | — |
| Product | HCID 66619688 | HCID 66619688 | 78% |
Reaction Steps
Methyl 4-(3-(trifluoromethylthio)phenylcarbamoyl)furan-3-carboxylate is prepared from 4-(methoxycarbonyl)furan-3-carboxylic acid and 3-(trifluoromethylthio) aniline following Method G (yield=78%). 1H NMR (300 MHz, CHCl3) δ 11.66 (s, 1H), 8.29 (s, 1H), 8.22-8.09 (m, 1H), 7.96-7.82 (m, 2H), 7.50-7.37 (m, 2H), 3.99 (s, 3H); ESI(−) calcd. for C14H9F3NO4S (344.02). Found 344.0
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08088804B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-557cbf7b56d349e6b8b02ad9bde101d1 |
| Source note | uspto-grants-2012_01 |