HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 136174321, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 59866349 | HCID 59866349 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 136174321 | HCID 136174321 | — |
Reaction Steps
1-(2-hydroxy-5-nonyl-phenyl)dodecane-1,3-dione (0.1 M) dissolved in ethanol (50 ml), hydrazine hydrate (0.105M) added and the reaction solution heated to reflux. Held at reflux for 2 hours, cooled to ambient and organic phase washed with water (2×25 ml). Toluene removed by vacuum evaporation to produce a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08088810B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-e0766be59bc64163a82779140fcc5e28 |
| Source note | uspto-grants-2012_01 |