HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 416033Generated: October 29, 2026
Hexamethylenetetramine → 3,5-Dimethyl-4-hydroxybenzaldehyde
https://huagongshe.com/reaction/416033
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hexamethylenetetramine | HCID 4101 | — |
| Reactant | 2,6-Dimethylphenol | HCID 11335 | — |
| Reactant | Acetic acid--water (1/1) | HCID 21899381 | — |
| Product | 3,5-Dimethyl-4-hydroxybenzaldehyde | HCID 75222 | — |
Reaction Steps
2,6-Dimethylphenol (0.34 g/mL) and hexamethylenetetramine (2 eq.) are dissolved in 2:1 acetic acid/water mixture. The whole is heated at 100° C. for 4 hours. The reaction mixture is cooled to room temperature and poured into a water/ice mixture. The precipitate is drained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08088819B2 |
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| Source dataset | uspto-grants-2012_01 |
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| ORD ID | ord-300642b878b346b08d52c741b67963bd |
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| Source note | uspto-grants-2012_01 |
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