huagongshe.com
HRID416049

反应详情

EQUATION

反应方程式

HRID 416049 的结构方程式

REACTANTS

反应物

2
结构：O=Cc1ccc(O)c(Cl)c1Cl
HCID528380

2,3-dichloro-4-hydroxybenzaldehyde

C7H4Cl2O2

结构：CC(=O)c1ccc(-c2ccc(OC(F)(F)F)cc2)s1
HCID59180351

未命名化合物

PRODUCTS

生成物

1
结构：O=C(C=Cc1ccc(O)c(Cl)c1Cl)c1ccc(-c2ccc(OC(F)(F)F)cc2)s1
HCID66623914

未命名化合物

PROCEDURE

实验过程

3-(2,3-Dichloro-4-hydroxyphenyl)-1-(5-(4-(trifluoromethoxy)phenyl)thien-2-yl)prop-2-en-1-one is prepared from 1-(5-(4-(trifluoromethoxy)phenyl)thien-2-yl)-ethanone and 2,3-dichloro-4-hydroxybenzaldehyde according to general procedure B. The evaporation residue is crystallized from acetonitrile.

WORKUP

后处理

  1. customThe evaporation residue is crystallized from acetonitrile