HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxy-3-methylbenzaldehyde → 3-(4-Hydroxy-3-methylphenyl)-1-(5-(4-(trifluoromethyl)phenyl)thien-2-yl)prop-2-en-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxy-3-methylbenzaldehyde | HCID 139901 | — |
| Reactant | 1-(5-(4-(Trifluoromethyl)phenyl)thiophen-2-yl)ethan-1-one | HCID 4191494 | — |
| Product | 3-(4-Hydroxy-3-methylphenyl)-1-(5-(4-(trifluoromethyl)phenyl)thien-2-yl)prop-2-en-1-one | HCID 66624025 | — |
Reaction Steps
3-(4-Hydroxy-3-methylphenyl)-1-(5-(4-(trifluoromethyl)phenyl)thien-2-yl)prop-2-en-1-one is prepared from 1-(5-(4-(trifluoromethyl)phenyl)thien-2-yl)ethanone and 4-hydroxy-3-methylbenzaldehyde according to general procedure B. The evaporation residue is washed with dichloromethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08088819B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-cac442d986954a10b0d48e9d6f6b45cd |
| Source note | uspto-grants-2012_01 |