Hydrazine → HCID 66625026, compound

Participants

Reaction Steps

2-Amino-ethanesulfonic acid (1-isopropyl-piperidin-4-yl)-thiazol-2-ylmethyl-amide was prepared by an analogous procedure as described for example 1 ii) starting from 178 mg (0.37 mmol) 2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethanesulfonic acid (1-isopropyl-piperidin-4-yl)-thiazol-2-ylmethyl-amide and 0.75 ml (2 equiv.) of a 1M hydrazine-solution in THF. The product was obtained as brown oil. Yield: 140 mg MS (ES+): m/e=347.

Provenance & Evidence