HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 22266503, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 22266527 | HCID 22266527 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22266503 | HCID 22266503 | — |
Reaction Steps
To a solution of 3-(benzoxazol-2-yloxymethyl)-1-butyl-2-pyridone (7-008-03) (169 mg) in methylene chloride (4.0 mL) was added thionyl chloride (122 mg) at room temperature. After stirring for 1 h, the solvent was removed to 1-butyl-3-chloromethyl-2-pyridone (7-008-04) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08088924B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-21c7abf0912e4c67b5a3160ebd64be6e |
| Source note | uspto-grants-2012_01 |