HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 41725Generated: October 29, 2026
Trifluoroacetic acid → HCID 86660476, compound
https://huagongshe.com/reaction/41725
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86660477 | HCID 86660477 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86660476 | HCID 86660476 | 99% |
Reaction Steps
TFA (1.6 ml) was dropped into an ice-cooled solution of octadeca-9,12-dienoic acid (E)-3-adamantan-1-yl-4′-(2-tert-butoxycarbonylvinyl)biphenyl-4-yl ester (110 mg, 0.159 mmol) in DCM (1.6 ml) and the resulting solution was stirred for 30 min at 0° C. The solvent was removed under reduced pressure to obtain the title compound as a white solid (100 mg, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08530517B2 |
|---|
| Source dataset | uspto-grants-2013_09 |
|---|
| ORD ID | ord-45c5b184600743c9a414bb750fa959a8 |
|---|
| Source note | uspto-grants-2013_09 |
|---|