HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycine tert-butyl ester → HCID 178446421, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycine tert-butyl ester | HCID 151417 | — |
| Reactant | 4-(Tert-butyl-dimethyl-silanyloxy)-3,3-dimethyl-butyraldehyde | HCID 10489671 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178446421 | HCID 178446421 | 100% |
Reaction Steps
In a manner similar to the method described in Example 1, glycine tert-butyl ester (0.52 g, 3.64 mmol) was reacted with 4-(tert-butyl-dimethyl-silanyloxy)-3,3-dimethyl-butyraldehyde (0.84 g, 3.64 mmol) in CH2Cl2 at room temperature for 18 h to give [4-(tert-butyl-dimethyl-silanyloxy)-3,3-dimethyl-but-(E)-ylideneamino]-acetic acid tert-butyl ester as a colorless oil (1.25 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08088815B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-44e06a76580445ff9b83958f8d601c96 |
| Source note | uspto-grants-2012_01 |