反应详情

温度

290 °C

A 0.5 inch (12.7 mm) by 40 inch (101.6 cm) plug flow reactor that is packed with Helipack Monel support is heated to 290° C. A 50/50 (molar %) mixture of hexafluoropropene and chloroform is fed into the reactor at about 1.5 g/min. The reactor pressure is maintained at 100 psig. The effluent from the reactor is fed into a distillation column and the unreacted reagents removed by distillation and recycled. The product CCl3CF2CHFCF3 is used in the next reaction.

1. temperatureThe reactor pressure is maintained at 100 psig
2. distillationThe effluent from the reactor is fed into a distillation column
3. customthe unreacted reagents removed by distillation
4. customThe product CCl3CF2CHFCF3 is used in the next reaction