Hydrochloric Acid → HCID 178516619, compound

HRID 41765Notes

Reaction equation

HRID 41765 reaction equation
[NH:1]1[C:5]2[CH:6]=[CH:7][C:8]([N:10]3[CH:14]([C:15]4[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=4)[C:13](=[O:21])[CH:12](C(OCC)=O)[C:11]3=[O:27])=[CH:9][C:4]=2[N:3]=[CH:2]1.Cl>>[NH:1]1[C:5]2[CH:6]=[CH:7][C:8]([N:10]3[CH:14]([C:15]4[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=4)[C:13](=[O:21])[CH2:12][C:11]3=[O:27])=[CH:9][C:4]=2[N:3]=[CH:2]1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 178470023HCID 178470023, compound

Product 1

HCID 178516619HCID 178516619, compound

Procedure

The compound was synthesized starting from ethyl 1-(1H-benzo[d]imidazol-5-yl)-2,4-dioxo-5-phenylpyrrolidine-3-carboxylate (which may be prepared in accordance with the procedure described for Intermediate 5; 0.1 g, 0.196 mmol) and 5 N aqueous hydrochloric acid (6 ml) according to the method described in Method 1, step 3.

Workup

  1. customThe compound was synthesized
  2. custommay be prepared in accordance with the procedure

Sources & evidence

ORD record
ord-ef83aa774eb245a8ba28fbee97ea7e11
Source dataset
uspto-grants-2013_09
Patent number
US08530670B2

Reaction notes

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