Hydrochloric Acid → HCID 66651457, compound

Participants

Reaction Steps

As described for Example 120, 238 mg of the polar diastereoisomer of 5-methyl-2-phenyl-2H-[1,2,3]triazole-4-carboxylic acid (4-dimethylamino-4-phenylcyclohexyl)amide were also obtained, which, dissolved in 5 ml 2-butanone and 5 ml ethyl acetate, were converted into the corresponding hydrochloride by adding 10.6 μl water, 75 μl chlorotrimethylsilane and 10 ml diisopropylether (165 mg of white solid).

Provenance & Evidence