HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 22467910, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 1,3-Dichloroacetone | HCID 10793 | — |
| Reactant | Thiourea | HCID 2723790 | — |
| Product | HCID 22467910 | HCID 22467910 | — |
Reaction Steps
A solution of 1,3-dichloroacetone (917 mg, 7.23 mmol) in acetone (6 mL) was added a solution of thiourea (550 mg, 7.23 mmol) in acetone (30 mL) at a fairly fast speed. The mixture was stirred at room temperature overnight. The formed solid was filtered and the filtrate was concentrated to give 524 mg of (2-amino-thiazol-4-yl)-methanol monohydrochloride as colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08093266B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-4d5ad3778dfd4039bcb41c0f107cbe1f |
| Source note | uspto-grants-2012_01 |