HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 854919-87-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 59845732 | HCID 59845732 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Product | 854919-87-2 | HCID 59845710 | — |
Reaction Steps
A mixture of 4,4-dimethyl-1-(nitromethyl)cyclohexanol (1.5 g, 0.0072 mol) and palladium hydroxide (0.1 g, 0.0001 mol) in methanol (50 mL, 1 mol) was stirred under hydrogen (1 atm) at room temperature overnight. The mixture was filtered and concentrated to afford the desired product as a clear oil. (1.08 g, 95%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08093265B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-90974ff8a87f410cbd97398b24b09c90 |
| Source note | uspto-grants-2012_01 |