HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyaniline → 1-(2-Methoxyphenylcarbamoyl)cyclopropanecarboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyaniline | HCID 7000 | — |
| Reactant | 1-(Phenylcarbamoyl)cyclopropanecarboxylic acid | HCID 19096871 | — |
| Product | 1-(2-Methoxyphenylcarbamoyl)cyclopropanecarboxylic acid | HCID 55035309 | 44% |
Reaction Steps
Following the procedure described above for the synthesis of compound 161 (Scheme 45), but replacing aniline for 2-methoxyaniline, title compound 172 was obtained in 44% yield. M/S (m/z): 236.0 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08093264B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-15ab14e4b7e44732b59a7694cef05636 |
| Source note | uspto-grants-2012_01 |