Sodium Bicarbonate → 2,6-Dibromo-4-methylbenzaldehyde [4-(methyloxy)phenyl]hydrazone

Participants

Reaction Steps

Sodium bicarbonate (0.84 g, 10 mmol) was added to a solution of 2,6-dibromo-4-methylbenzaldehyde (2.62 g, 9.43 mmol) and [4-(methyloxy)phenyl]hydrazine hydrochloride (1.65 g, 9.45 mmol) in methanol (60 mL) and the mixture heated under reflux for 15 min. The mixture was then cooled and evaporated to give the crude title compound which was used without purification.

Provenance & Evidence