反应详情

Sodium bicarbonate (0.84 g, 10 mmol) was added to a solution of 2,6-dibromo-4-methylbenzaldehyde (2.62 g, 9.43 mmol) and [4-(methyloxy)phenyl]hydrazine hydrochloride (1.65 g, 9.45 mmol) in methanol (60 mL) and the mixture heated under reflux for 15 min. The mixture was then cooled and evaporated to give the crude title compound which was used without purification.

1. temperaturethe mixture heated
2. temperatureunder reflux for 15 min
3. temperatureThe mixture was then cooled
4. customevaporated