HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Iodo-5-isopropoxy-4-methoxyphenyl)ethanol → 2'-Iodo-5'-isopropoxy-4'-methoxyacetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Iodo-5-isopropoxy-4-methoxyphenyl)ethanol | HCID 66761030 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | 2'-Iodo-5'-isopropoxy-4'-methoxyacetophenone | HCID 66761117 | — |
Reaction Steps
Concentration of fraction B (Rf 0.6 in 1:1 v/v ethyl acetate/hexane) afforded the starting alcohol 6 (200 mg, 19% recovery) as a pale-yellow oil that was identical, as judged by 1H NMR spectroscopic analysis, with authentic material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536157B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-3f9e0455cb2c4997a7de0f7bd264406a |
| Source note | uspto-grants-2013_09 |