HuagongsheHuagongshe Chemistry Print Report · For research reference only
3'-Isopropoxy-4'-methoxypropiophenone → 3'-Hydroxy-4'-methoxypropiophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3'-Isopropoxy-4'-methoxypropiophenone | HCID 66760948 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | 3'-Hydroxy-4'-methoxypropiophenone | HCID 919755 | — |
Reaction Steps
Concentration of fraction B (Rf 0.6 in 1:1 v/v ethyl acetate/hexane) afforded the starting ether 10 (207 mg, 50% recovery) as a white solid that was identical, as judged by 1H NMR spectroscopic analysis, with authentic material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536157B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-1fcc45850ae64be1a8e1913d412d0ca8 |
| Source note | uspto-grants-2013_09 |