HuagongsheHuagongshe Chemistry Print Report · For research reference only
2'-Iodo-5'-isopropoxy-4'-methoxypropiophenone → 5'-Hydroxy-2'-iodo-4'-methoxypropiophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2'-Iodo-5'-isopropoxy-4'-methoxypropiophenone | HCID 66761045 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | 5'-Hydroxy-2'-iodo-4'-methoxypropiophenone | HCID 66760961 | — |
Reaction Steps
Concentration of fraction B (Rf 0.7 in 1:1 v/v ethyl acetate/hexane) afforded the starting ether 11 (98 mg, 21% recovery) as a pale-yellow oil that was identical, as judged by 1H NMR spectroscopic analysis, with authentic material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536157B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-4ae90d36c96c48969af44e062cb22feb |
| Source note | uspto-grants-2013_09 |