Sodium Hydroxide → HCID 66651500, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of EXAMPLE 1B (7.1 g) in ethanol (26 mL) was added 30% sodium hydroxide (17.63 mL) and the mixture was stirred for 5 minutes. Water (35 mL) was added and 4 mL aliquots of the mixture were added at 1-minute intervals to a heated (85° C.) solution of potassium ferricyanide(III) (29 g) in water (260 mL). The mixture was maintained at 85° C. for 30 minutes and cooled. The precipitate was collected, washed with water and dried to afford the title compound.

Provenance & Evidence