HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66649236, compound → HCID 66649563, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66649236 | HCID 66649236 | — |
| Solvent | Ammonia | HCID 222 | — |
| Product | HCID 66649563 | HCID 66649563 | 84% |
Reaction Steps
A solution of compound 51 (500 mg, 0.84 mmol) in saturated methanolic ammonia (10 mL) was stirred at room temperature for 24 hr, concentrated to dryness, washed with EtOAc several times, and dried to give 52 (200 mg, 84%) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08093380B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-5511c2c2490f4d8a902387371d77f908 |
| Source note | uspto-grants-2012_01 |