Pentane → HCID 86643015, compound
Reaction equation
[C:1]([F:5])([CH3:4])([CH3:3])[CH3:2].[CH3:6][CH2:7][CH2:8][CH2:9][CH3:10]>>[C:1]([F:5])([CH3:4])([CH3:3])[CH3:2].[CH3:6][CH2:7][CH2:8][CH2:9][CH3:10]Participants
3
Procedure
500 mL of cold n-pentane kept at 0° C. was poured in a glass graduated cylinder. To the n-pentane was added 2.3 mL of tert-butyl fluoride also kept at 0° C. The resulting solution was thoroughly mixed and analyzed by CAP-GC by the CGSB method for gasoline. The concentration of the tert-butyl fluoride was found to be 0.43 wt %. The solution was kept in the refrigerator at 0° C.
Workup
- customkept at 0° C.
- additionwas poured in a glass
- customalso kept at 0° C
- additionThe resulting solution was thoroughly mixed
- customwas kept in the refrigerator at 0° C.
Sources & evidence
- ORD record
- ord-44fecbb94efb47f0a208885fa5437c5c
- Source dataset
- uspto-grants-2012_01
- Patent number
- US08093441B2
Reaction notes
Loading…