HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 57586542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Reactant | HCID 57586478 | HCID 57586478 | — |
| Product | HCID 57586542 | HCID 57586542 | 78% |
Reaction Steps
A similar procedure as described in Example 12, step 5 was used, starting from 3′-fluoro-5-methoxy-biphenyl-3-ylamine (940 mg, 4.32 mmol), sodium nitrite (545 mg, 7.79 mmol), and potassium iodide (1.44 mg, 8.65 mmol) to afford 3′-fluoro-3-iodo-5-methoxy-biphenyl (1.1 g, 78%) as an amorphous light yellow oil: ES(+)-HRMS m/e calculated for C13H10FIO (M+H)+ 329.1190, found 329.1192.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08093385B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-4047dbda1ba4442aa969b21db34e97ff |
| Source note | uspto-grants-2012_01 |