HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Bromophenyl)-1-phenyl-1H-benzo(d)imidazole → 2-[5-(10-naphthalene-2-yl-anthracene-9-yl)-pyridine-3-yl]-1-phenyl-1H-benzimidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Bromophenyl)-1-phenyl-1H-benzo(d)imidazole | HCID 23094070 | — |
| Reactant | 2-(5-bromopyridine-3-yl)-1-phenyl-1H-benzimidazole | HCID 23094085 | — |
| Product | 2-[5-(10-naphthalene-2-yl-anthracene-9-yl)-pyridine-3-yl]-1-phenyl-1H-benzimidazole | HCID 86643772 | — |
Reaction Steps
Almost the same procedure as step (2) in Synthesis Example 1 was carried out except that corresponding 2-(5-bromopyridine-3-yl)-1-phenyl-1H-benzimidazole was used instead of 2-(4-bromophenyl-phenyl-1H-benzimidazole, resultantly obtaining an aimed compound (Compound (4-6) (yield: 36%). As a result of MS analysis, it was recognized that m/e=573 for aimed substance's molecular weight of 573.22.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08097349B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-8b75b90c79ba4e308c354d7609e2b5dc |
| Source note | uspto-grants-2012_01 |