HRID420598

反应详情

EQUATION

反应方程式

HRID 420598 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 2-(1-benzyl-4-pyrrolidine-1-ylpiperidine-4-yl)ethanol (9.28 g), 10% Pd/C (1.86 g) and methanol (100 mL) was stirred under hydrogen (4 atm) for 3 days. The insoluble material was filtrated and the filtrate was concentrated to give the title compound (6.30 g).

WORKUP

后处理

  1. filtrationThe insoluble material was filtrated
  2. concentrationthe filtrate was concentrated