HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 66657906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Tert-butyl 4-cyanopiperidine-1-carboxylate | HCID 1514443 | — |
| Product | HCID 66657906 | HCID 66657906 | 99% |
Reaction Steps
4-Cyanopiperidine-1-carboxylic acid t-butyl ester (5.35 g) was added to trifluoroacetic acid (20 mL) and the mixture was stirred at room temperature for 10 minutes. Trifluoroacetic acid was evaporated under reduced pressure to give the title compound as colorless crystal (5.62 g). Yield: 99%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08097610B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-03aefceb38424f8a853e89004b7efc01 |
| Source note | uspto-grants-2012_01 |