HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67394387, compound → HCID 66766326, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67394387 | HCID 67394387 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 66766326 | HCID 66766326 | 62% |
Reaction Steps
The solid residue obtained in step A was dissolved in 3 ml of trifluoroacetic acid and stirred for 1 hour at room temperature. The solvent was evaporated and the solid residue was triturated with an isopropyl ether/hexane mixture. The solid was filtered off affording 0.16 g (yield 62%) of the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536165B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-9024398e87ca43078c2ab2325cb941aa |
| Source note | uspto-grants-2013_09 |