HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67394347, compound → 2-((5,6-Difluoropyridin-3-yl)amino)-5-methylbenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67394347 | HCID 67394347 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | 2-((5,6-Difluoropyridin-3-yl)amino)-5-methylbenzoic acid | HCID 46847515 | 15% |
Reaction Steps
The solid residue obtained in step A was dissolved in 0.78 ml of trifluoroacetic acid and stirred for 1 hour at room temperature. The solvent was evaporated and the solid residue was triturated with an isopropyl ether/hexane mixture. The solid was filtered off affording 0.01 g (yield 15%) of the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536165B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-5a43acfad05a4d7181afe9d1c0bd7baa |
| Source note | uspto-grants-2013_09 |