HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 46847798, compound → 2-(6-(3-Cyclopropoxyphenyl)-5-methylpyridin-3-ylamino)-5-methylbenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 46847798 | HCID 46847798 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | 2-(6-(3-Cyclopropoxyphenyl)-5-methylpyridin-3-ylamino)-5-methylbenzoic acid | HCID 46847797 | 74% |
Reaction Steps
The solid residue obtained in step A was dissolved in 1.5 ml of trifluoroacetic acid and stirred for 45 minutes at room temperature. The solvent was evaporated and the solid residue was tritured with a diethyl ether/hexane mixture. The solid was filtered off affording 0.093 g (yield 74%) of the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536165B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-cd5d4032ec684a0fa651815938f396a6 |
| Source note | uspto-grants-2013_09 |