HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → 2-Propenoic acid, 2-(phenylthio)ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Hydroxyethyl benzene thiol | HCID 11240608 | — |
| Reactant | Chloride acrylate | HCID 21924244 | — |
| Product | 2-Propenoic acid, 2-(phenylthio)ethyl ester | HCID 22676929 | 80% |
Reaction Steps
60 g of hydroxyethyl benzene thiol and 44.7 g of chloride acrylate were reacted in 244 g of pyridine at 25° C. for 4 hours and then formed by distillation into 2-(phenylthio)ethyl acrylate with 80% yield. A synthetic monomer 6 was obtained with 82% yield in the same manner as in Synthesis Example 1 except that 2-(phenylthio)ethyl acrylate was used in place of phenoxyethyl acrylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08097688B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-36b75d901a2c4e6bb85a97f739ab32ee |
| Source note | uspto-grants-2012_01 |