3-Hydroxy-2-naphthoic acid → HCID 9973986, compound
Reaction equation
[OH:1][C:2]1[C:3]([C:12]([OH:14])=O)=[CH:4][C:5]2[C:10]([CH:11]=1)=[CH:9][CH:8]=[CH:7][CH:6]=2.[Cl:15][C:16]1[CH:17]=[C:18]([CH:20]=[C:21]([Cl:23])[CH:22]=1)[NH2:19]>>[Cl:15][C:16]1[CH:17]=[C:18]([NH:19][C:12]([C:3]2[C:2]([OH:1])=[CH:11][C:10]3[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=3)[CH:4]=2)=[O:14])[CH:20]=[C:21]([Cl:23])[CH:22]=1Participants
3
Procedure
Using 3-hydroxynaphthalene-2-carboxylic acid and 3,5-dichloroaniline as the raw materials, the same operation as the example 16 gave the title compound.
Sources & evidence
- ORD record
- ord-30a47d6938494397843e3029a55a9642
- Source dataset
- uspto-grants-2012_01
- Patent number
- US08097759B2
Reaction notes
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