HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57639405, compound → HCID 57639279, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57639405 | HCID 57639405 | — |
| Reactant | HCID 66672674 | HCID 66672674 | — |
| Product | HCID 57639279 | HCID 57639279 | 57% |
Reaction Steps
The title compound was prepared as (4S)-4-{2-[(methylethyl)amino]-8-[(2,4,6-trifluorophenyl)amino]purin-9-yl}pentanamide with methyl (4R)-4-{2-[(methylethyl)amino]-8-[(2,4,6-trifluorophenyl)amino]purin-9-yl}pentanoate (500 mg, 1.15 mmol) to give the title compound (273 mg, 57%): ES-MS (m/z) 422.3 [M+1]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101588B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-9f7e7391822d42d8972223628f610477 |
| Source note | uspto-grants-2012_01 |