huagongshe.com
HRID421695

反应详情

EQUATION

反应方程式

HRID 421695 的结构方程式

REACTANTS

反应物

2
结构：C1CCNCC1
HCID8082

Piperidine

C5H11N

结构：O=C(Nc1ccc(Cl)c(NC(=O)c2ccccc2)c1)c1ccc(CBr)nc1
HCID16730952

未命名化合物

PRODUCTS

生成物

1
结构：O=C(Nc1ccc(Cl)c(NC(=O)c2ccccc2)c1)c1ccc(CN2CCCCC2)nc1
HCID16731029

未命名化合物

PROCEDURE

实验过程

N-(3-benzamido-4-chlorophenyl)-6-(bromomethyl)nicotinamide (0.11 mmol) was used in general procedure 5 with piperidine (0.12 mmol). The product was purified by RP-HPLC to give N-(3-benzamido-4-chlorophenyl)-6-(piperidin-1-ylmethyl)nicotinamide. MS (Q1) 448.1 (M)+

WORKUP

后处理

  1. customThe product was purified by RP-HPLC