HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Acetylpiperazine → 2-Methylnicotinamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Acetylpiperazine | HCID 83795 | — |
| Reactant | HCID 16730160 | HCID 16730160 | — |
| Product | 2-Methylnicotinamide | HCID 12243705 | — |
Reaction Steps
6-chloro-N-(4-chloro-3-(3-chlorobenzamido)phenyl)-2-methylnicotinamide (0.16 mmol) was used in general procedure 3 with 1-acetylpiperazine (0.83 mmol). The product was purified by RP-HPLC to give 6-(4-acetylpiperazin-1-yl)-N-(4-chloro-3-(3-chlorobenzamido)phenyl))phenyl)-2-methylnicotinamide. MS (Q1) 526.1 (M)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101610B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-51c013fc20874a959b616eb984f66299 |
| Source note | uspto-grants-2012_01 |