HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59804293, compound → HCID 59804362, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59804293 | HCID 59804293 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59804362 | HCID 59804362 | — |
Reaction Steps
To a solution of [2-nitro-5-(3-nitro-phenylamino)-phenyl]-acetic acid ethyl ester (0.36 g, 1.0 mmol) in methanol (10 ml) is added Pd/C (10%, wet, 0.1 g). The reaction is placed under a hydrogen balloon and stirred for 20 hours. The catalyst is filtered and the solvent is removed to give the desired compound. LC-MS: 286.1 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101608B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-f19e19ac5cc6404d807670efe283fc57 |
| Source note | uspto-grants-2012_01 |