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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 422027Generated: November 1, 2026

HCID 59804293, compound → HCID 59804362, compound

https://huagongshe.com/reaction/422027

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59804293HCID 59804293—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 59804362HCID 59804362—

Reaction Steps

To a solution of [2-nitro-5-(3-nitro-phenylamino)-phenyl]-acetic acid ethyl ester (0.36 g, 1.0 mmol) in methanol (10 ml) is added Pd/C (10%, wet, 0.1 g). The reaction is placed under a hydrogen balloon and stirred for 20 hours. The catalyst is filtered and the solvent is removed to give the desired compound. LC-MS: 286.1 (MH+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08101608B2
Source datasetuspto-grants-2012_01
ORD IDord-f19e19ac5cc6404d807670efe283fc57
Source noteuspto-grants-2012_01