HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetophenone → HCID 86633655, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetophenone | HCID 7410 | — |
| Reactant | 4-Fluoro-3-methylbenzoic acid | HCID 242828 | — |
| Reactant | 4-(4-fluoro-3-methylphenyl)-6-phenylpyrimidin-2(1H)-one | HCID 16660661 | — |
| Reactant | Methyl 2-(2-methoxyethoxy)benzoate | HCID 22381872 | — |
| Product | HCID 86633655 | HCID 86633655 | — |
Reaction Steps
Using the same or analogous synthetic techniques described in Example 1, 4-(4-fluoro-3-methylphenyl)-6-phenylpyrimidin-2(1H)-one was prepared by replacing 1-[(4-hydroxy-3-methyl)phenyl]ethanone with commercially available acetophenone and methyl 2-{[2-(methyloxy)ethyl]oxy}benzoate with commercially available 4-fluoro-3-methylbenzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101625B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-4ece72248d834bc68264202605078eec |
| Source note | uspto-grants-2012_01 |