HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dichlorobenzaldehyde → 4-(4-Hydroxy-3-methylphenyl)-6-[2-(1-methylethyl)phenyl]pyrimidin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dichlorobenzaldehyde | HCID 35745 | — |
| Reactant | 2-(Propan-2-yl)benzaldehyde | HCID 590536 | — |
| Reactant | 4-(4-hydroxy-3-methylphenyl)-6-[2-(1-methylethyl)phenyl]pyrimidin-2(1H)-one | HCID 135589861 | — |
| Product | 4-(4-Hydroxy-3-methylphenyl)-6-[2-(1-methylethyl)phenyl]pyrimidin | HCID 136356808 | — |
Reaction Steps
Using the same or analogous synthetic techniques described in Example 68, 4-(4-hydroxy-3-methylphenyl)-6-[2-(1-methylethyl)phenyl]pyrimidin-2(1H)-one was prepared by replacing 2,3-dichlorobenzaldehyde with commercially available 2-isopropylbenzaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101625B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-5ae823fd763547d3b700ea1f030fb04a |
| Source note | uspto-grants-2012_01 |