HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 25017037, compound → HCID 66672330, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 25017037 | HCID 25017037 | — |
| Reactant | HCID 86637281 | HCID 86637281 | — |
| Product | HCID 66672330 | HCID 66672330 | — |
Reaction Steps
Following the procedure of Example 3, but substituting (R)-2-(4-chlorophenyl)-5-(1-(2-(3-hydroxypyrrolidin-1-yl)ethyl)-1H-indazol-5-yl)furo[3,2-c]pyridine-4-one for the (R)-2-(4-chlorophenyl)-5-(1-(2-(2-hydroxymethyl)pyrrolidin-1-yl)ethyl)-1H-indazol-5-yl)furo[3,2-c]pyridine-4-one, the title compound (22.2 mg, quantitative) was prepared as an off-white solid: mp 242-246° C. (decomposition); ESI MS m/z 475 [M+H]+; HPLC (Method A) 97.6% (AUC), tR=15.4 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101632B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-21de86920a03403ab364073dea8deb03 |
| Source note | uspto-grants-2012_01 |