HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 59240564, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 2-[4-(4-Benzyl-phthalazin-1-yl)-piperazin-1-yl]-pyrimidin-5-ylamine | HCID 59240578 | — |
| Product | HCID 59240564 | HCID 59240564 | 31.9% |
Reaction Steps
Following the above procedure, 2-[4-(4-Benzyl-phthalazin-1-yl)-piperazin-1-yl]-pyrimidin-5-ylamine (60 mg, 0.15 mmol) and acetic anhydride (22.2 μL, 0.235 mmol) afford the title compound (21 mg, 31%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536168B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-ef8fd8292a4f416282afbb4b84638556 |
| Source note | uspto-grants-2013_09 |