Thionyl Chloride → HCID 59750697, compound

Participants

Reaction Steps

Charge flask with 6-(5-Hydroxy-5,6,7,8-tetrahydro-naphthalen-2-yloxy) nicotinamide (288 mg, 1.01 mmol) and SOCl2 (5 ml) and beat at 50° C. under nitrogen atmosphere with stirring. After 3.5 hours, concentrate on rotary evaporator to give the title compound as a yellow oil. Due to instability, use this material without purification.

Provenance & Evidence