HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-3-fluoropyridine → HCID 66598099, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-3-fluoropyridine | HCID 2782791 | — |
| Reactant | HCID 86086817 | HCID 86086817 | — |
| Product | HCID 66598099 | HCID 66598099 | 13.1% |
Reaction Steps
According to the protocol described in Example 237(B), the reaction between 3-chlorophenyl pent-4-ynoate (580 mg, 2.80 mmol) and 2-chloro-3-fluoropyridine (370 mg, 2.80 mmol) afforded 111 mg of 3-chlorophenyl 5-(3-fluoropyridin-2-yl)pent-4-ynoate (Yield: 13%) as yellow-oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101637B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-0b23843ff5174258b5f8491e8b469a2c |
| Source note | uspto-grants-2012_01 |