HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,4,5,5-Tetramethyl-2-(2-methyl-4-(trifluoromethylsulfonyl)phenyl)-1,3,2-dioxaborolane → Methyl 4-methyl-3-(1-(2-methyl-4-(trifluoromethylsulfonyl)phenyl)phthalazin-6-yl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,4,5,5-Tetramethyl-2-(2-methyl-4-(trifluoromethylsulfonyl)phenyl)-1,3,2-dioxaborolane | HCID 59594186 | — |
| Reactant | Methyl 3-(1-chlorophthalazin-6-yl)-4-methylbenzoate | HCID 77230175 | — |
| Product | Methyl 4-methyl-3-(1-(2-methyl-4-(trifluoromethylsulfonyl)phenyl)phthalazin-6-yl)benzoate | HCID 66674278 | — |
Reaction Steps
Methyl 4-methyl-3-(1-(2-methyl-4-(trifluoromethylsulfonyl)phenyl)phthalazin-6-yl)benzoate was prepared according to the procedure described in Example 223, using 4,4,5,5-tetramethyl-2-(2-methyl-4-(trifluoromethylsulfonyl)phenyl)-1,3,2-dioxaborolane and methyl 3-(1-chlorophthalazin-6-yl)-4-methylbenzoate as starting materials. MS (ESI, pos. ion) m/z: 500.9 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101612B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-fbf78b296b63491d84d1138f5cca5b1b |
| Source note | uspto-grants-2012_01 |