Phenol → HCID 25267396, compound

Participants

Reaction Steps

The title compound 448 was synthesized starting from compound 32 using the procedure F as described for the synthesis of phenol 807. 1H-NMR (400 MHz, CDCl3): δ ppm 7.18-7.07 (m, 2H), 6.82 (dt, J=8.79, 8.79, 2.75 Hz, 1H), 6.78-6.69 (m, 3H), 6.62 (dd, J=8.20, 2.73 Hz, 1H), 5.08 (broad s, 1H), 4.91 (dd, J=7.30, 1.61 Hz, 1H), 2.45-2.26 (m, 1H), 2.23-1.95 (m, 2H), 1.82 (tdd, J=14.57, 12.67, 1.56, 1.56 Hz, 1H), 1.77-1.48 (m, 4H), 1.44-1.03 (m, 2H).

Provenance & Evidence