HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57701070, compound → HCID 25267399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57701070 | HCID 57701070 | — |
| Reactant | HCID 57701091 | HCID 57701091 | — |
| Product | HCID 25267399 | HCID 25267399 | — |
Reaction Steps
The title compound 961 was synthesized from compound 34 (10 mg) using the procedure described for the synthesis of compound 20. Purity LC MS/UV: m/z=265 (M−1) was confirmed. Yield: 7 mg (93%). 1H-NMR (400 MHz, CDCl3): δ ppm 7.26-7.20 (m, 2H), 7.17-7.11 (m, 1H), 6.87-6.84 (m, 3H), 6.80-6.77 (m, 2H), 4.83 (t, J=4.29, 4.29 Hz, 1H), 4.67 (s, 1H), 2.35-2.22 (m, 1H), 2.05-1.96 (m, 1H), 1.86-1.50 (m, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101651B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-fd4d104eb5844e268a1a6d4c293b9821 |
| Source note | uspto-grants-2012_01 |