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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 422886Generated: October 31, 2026

HCID 57701070, compound → HCID 25267399, compound

https://huagongshe.com/reaction/422886

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57701070HCID 57701070—
ReactantHCID 57701091HCID 57701091—
ProductHCID 25267399HCID 25267399—

Reaction Steps

The title compound 961 was synthesized from compound 34 (10 mg) using the procedure described for the synthesis of compound 20. Purity LC MS/UV: m/z=265 (M−1) was confirmed. Yield: 7 mg (93%). 1H-NMR (400 MHz, CDCl3): δ ppm 7.26-7.20 (m, 2H), 7.17-7.11 (m, 1H), 6.87-6.84 (m, 3H), 6.80-6.77 (m, 2H), 4.83 (t, J=4.29, 4.29 Hz, 1H), 4.67 (s, 1H), 2.35-2.22 (m, 1H), 2.05-1.96 (m, 1H), 1.86-1.50 (m, 6H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08101651B2
Source datasetuspto-grants-2012_01
ORD IDord-fd4d104eb5844e268a1a6d4c293b9821
Source noteuspto-grants-2012_01