HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2S)-2-[(1,1-Dimethylethoxy)methyl]oxirane → HCID 66676935, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2S)-2-[(1,1-Dimethylethoxy)methyl]oxirane | HCID 11768605 | — |
| Reactant | 2-Propanol, 2-methyl-, lithium salt (1:1) | HCID 23664764 | — |
| Reactant | HCID 131729414 | HCID 131729414 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 66676935 | HCID 66676935 | — |
Reaction Steps
Using N,N-dimethylformamide solution of isobutyl-2-(2-methoxyphenoxy)ethylcarbamate 26.7 g (0.1 mol), lithium-t-butoxide 1.60 g (0.02 mol) and (S)-2-t-butoxymethyl-oxiran 14.3 g (0.11 mol), the procedures as described in Example 1 were carried out to obtain the targeted product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101781B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-58c57d3cdd4c43489cc87d9d16042802 |
| Source note | uspto-grants-2012_01 |